[Pd(NCOC2H4CO)(PPh3)2Br]

[Pd(NCOC2H4CO)(PPh3)2Br] - Names and Identifiers

Name	BROMOBIS(PH3P)(N-SUCCINIMIDE)PD(II)
Synonyms	[Pd(NCOC2H4CO)(PPh3)2Br] BROMOBIS(PH3P)(N-SUCCINIMIDE)PD(II) bromo(n-succinimidyl)bis(triphenylphosphine)palladium(ii) trans-Bromo(N-succinimidyl)bis(triphenylphosphine)palladium(II) bromopalladium, pyrrolidin-1-ide-2,5-dione, triphenylphospho...
CAS	251567-28-9

[Pd(NCOC2H4CO)(PPh3)2Br] - Physico-chemical Properties

Molecular Formula	C40H34BrNO2P2Pd
Molar Mass	808.975
Melting Point	223-228 °C (dec.) (lit.)
Storage Condition	2-8℃

[Pd(NCOC2H4CO)(PPh3)2Br] - Risk and Safety

WGK Germany

[Pd(NCOC2H4CO)(PPh3)2Br] - Introduction

BROMOBIS(PH3P)(N-SUCCINIMIDE)PD(II), chemical formula Br[Pd(PPh3)2(N-Succinimide)], is an organometallic compound. The following is an introduction to its nature, use, preparation and safety information:

Nature:
1. Appearance: common orange-red solid;
2. Solubility: high solubility in organic solvents, such as chloroform, toluene, etc;
3. Thermal stability: high thermal stability, suitable for high temperature reaction conditions.

Use:
1. Catalyst: commonly used in organic synthesis, such as hydrogenation reaction, coupling reaction and redox reaction;
2. Transfer hydrogenation: applicable to the reduction of aldehydes and ketones;
3. Selective catalysis: can be used for the addition reaction of aldehydes and olefins.

Method:
The compound can be prepared by the following steps:
1. Adding palladium chloride (PdCl2) and N-succinimide (N-Succinimide) in toluene solvent, and reacting under the condition of stirring and heating;
2. Add triphenylphosphine (PPh3), continue stirring and heating reaction;
3. Finally, a bromine source (such as dibromoethane) is added into the reaction system to continue the reaction;
4. Filter and cool the solution to give BROMOBIS(PH3P)(N-SUCCINIMIDE)PD(II).

Safety Information:
1. The compound in the eye and skin contact may cause allergic reaction, should pay attention to personal protection;
2. Avoid inhaling dust or solution during operation;
3. It has a certain toxicity, should be properly preserved and handled, to avoid contact with the oxidant;
4. Should be operated in a well-ventilated laboratory and comply with chemical safety procedures.

Last Update：2024-04-10 22:29:15